Surface Analysis

For a surface sensitive chemical analysis our X-ray excited photoelectron spectroscopy supports you. The method is well-suited for a non-destructive (depth) analysis down to 10 nm. Primarily, semiconducting and metallic materials, as well as, their oxides are investigated. The sample preparation of organic and metallic thin films under ultra-high vacuum conditions is also possible and part of the service.

Technical data

PHI Spectrometer with 150mm hemispherical analyser
16 Slot Multi-channeltron Detector
Monochromated Al K(alpha) X-ray source
Switchable X-ray source with Al- and Mg-Anodes
Ultra-high vacuum and x-ray resistant
Solid, dry samples as bulk pellets, thin films or powders
Recommended size for compacted samples: max. 20 mm diameters and 10 mm thickness
Analysis (Elements from Li or above) of elemental composition and their detailed chemical binding states
Investigation of depth profiling of the elemental composition by repeatedly sputtering down to 500nm
Non-destructive layered structure analysis by angle dependent XPS down to 10nm ( suitable for natural oxide layers)
Valence state analysis for conducting samples with Helium discharge light source
Thin film preparation of metallic (DC-sputtering) or organic (sublimation) thin films under ultra-high vacuum conditions in separate preparation chambers